Highlights from the Lipid Analysis Literature - 1990

The following references were collected as part of a weekly literature search that reflects my (former) personal research interests. However, most mainstream lipid analytical topics are covered. Among the exceptions are "steroidal hormones", "prostanoids", "fat-soluble vitamins" and "terpenoids", although some papers in these categories may be posted. My intention is to list only those papers that exhibit novel analytical methodology as opposed to tried and tested methods, although this may appear to introduce a bias towards modern mass spectrometry techniques. References are listed alphabetically by the first author.

Ackman,R.G., McLeod,C.A. and Banerjee,A.K. An overview of analyses by Chromarod-Iatroscan TLC-FID. Appendix: Analytical applications. J. Planar Chromatogr. - Mod. TLC, 3, 450-490 (1990).
Adams,J. Charge-remote fragmentations: analytical applications and fundamental studies. Mass Spectrom. Rev., 9, 141-186 (1990).
Aitzetmuller,K. Flow gradients in the HPLC of triacylglycerols in fats and oils. J. High Resolut. Chromatogr., 13, 375-377 (1990).
Aitzetmuller,K. and Guaraldo Goncalves,L.A. Dynamic impregnation of silica stationary phases for the argentation chromatography of lipids. J. Chromatogr. A, 519, 349-358 (1990).
Albers,J.J., Marcovina,S.M. and Lodge,M.S. The unique lipoprotein(a): properties and immunochemical measurement. Clin. Chem., 36, 2019-2026 (1990).
Allen,K.G.D., Huang,C-J. and Morin,C.L. Determination of picomole quantities of hydroperoxides by a coupled glutathione peroxidase and glutathione disulfide specific glutathione reductase assay. Anal. Biochem., 186, 108-111 (1990).
Allenmark,S., Chelminska-Bertilsson,M. and Thompson,R.A. N-(9-Acridinyl)-bromoacetamide - a powerful reagent for phase-transfer-catalyzed fluorescence labelling of carboxylic acids for liquid chromatography. Anal. Biochem., 185, 279-285 (1990).
Allmaier,G., Schmid,E.R., Gasser,H., Strohmeier,W. and Schlag,G. Methodological approach to the characterization of diacylphosphatidylcholines in rabbit lung lavage fluid by FAB MS. Rapid Commun. Mass Spectrom., 4, 19-23 (1990).
Almog,R., Anderson-Samsonoff,C.A., Berns,D.S. and Saulsbery,R. A methodology for determination of phospholipids. Anal. Biochem., 188, 237-242 (1990).
Aloisi,J.D., Sherma,J. and Fried,B. Comparison of mobile phases for separation and quantification of lipids by one-dimensional TLC on preabsorbent high performance silica J. Liqu. Chromatogr., 13, 3949-3961 (1990).
Alvarez,J.G., Cazes,J., Touchstone,J.C. and Grob,R.L. Isolation and purification of lipids by centrifugal partition chromatography. J. Liqu. Chromatogr., 13, 3603-3614 (1990).
Alvarez,J.G., Storey,B.T., Hemling,M.L. and Grob,R.L. High-resolution proton NMR characterization of seminolipid from bovine spermatozoa. J. Lipid Res., 31, 1073-1081 (1990).
Amari,J.V., Brown,P.R., Grill,C.M. and Turcotte,J.G. Isolation and purification of lecithin by preparative HPLC. J. Chromatogr. A, 517, 219-228 (1990).
Araki,N., Horiuchi,S., Rahim,A.T.M.A., Takata,K. and Morino,Y. Microquantification of cholesterol and cholesteryl esters in rat peritoneal macrophages by reverse-phase HPLC. Anal. Biochem., 185, 339-345 (1990).
Auerbach,B.J., Parks,J.S. and Applebaum-Bowden,D. A rapid and sensitive micro-assay for the enzymatic determination of plasma and lipoprotein cholesterol. J. Lipid Res., 31, 738-742 (1990).
Azerad,R., Boucher,J.L., Dansette,P. and Delaforge,M. HPLC separation of 11-hydroxylauric acid enantiomers. Application to the determination of the stereochemistry of microsomal lauric acid (w-1)hydroxylation. J. Chromatogr. A, 498, 293-302 (1990).
Baba,N., Tateno,K., Iwasa,J. and Oda,J. Lipase-catalysed kinetic resolution of racemic methyl 13-hydroperoxy-9Z,11E-octadecadienoate in an organic solvent. Agric. Biol. Chem., 54, 3349-3350 (1990).
Baer,A.N., Costello,P.B. and Green,F.A. Characterization of the chirality of the monohydroxyeicosatetraenoic acids produced by rat basophilic leukemia cells. Biochem. Biophys. Res. Commun., 169, 332-338 (1990).
Baer,A.N., Costello,P.B. and Green,F.A. Free and esterified 13(R,S)-hydroxyoctadecadienoic acids: principal oxygenase products in psoriatic skin scales. J. Lipid Res., 31, 125-130 (1990).
Balazy,M., Cluzel,J. and Bazan,N.G. A novel method for the analysis of PAF and alkyl ether phospholipids by mass spectrometry. Adv. Prostaglandins, Thromboxanes, Leukotriene Res., 21, 323-326 (1990).
Baldwin,M.A., Stahl,N., Burlingame,A.L. and Prusiner,S.B. Structure determination of glycoinositol phospholipid anchors by permethylation and tandem MS. Methods (San Diego), 1, 306-314 (1990).
Bartlett,K., Hovik,R., Eaton,S., Watmough,N.J. and Osmundsen,H. Intermediates of peroxisomal beta-oxidation. A study of the fatty acyl-CoA esters which accumulate during peroxisomal beta-oxidation of [U-14C]hexadecanoate. Biochem. J., 270, 175-180 (1990).
Beare-Rogers,J.L. and Dieffenbacher,A. Determination of n-3 and n-6 unsaturated fatty acids in vegetable oils and fats by capillary GLC. Results of a collaborative study and the standardized method. Pure Appl. Chem., 62, 795-802 (1990).
Becart,J., Chevalier,C. and Biesse,J.P. Quantitative analysis of phospholipids by HPLC with a light-scattering detector - application to raw materials for cosmetic use. J. High Resolut. Chromatogr., 13, 126-129 (1990).
Bell,M.V. and Dick,J.R. Molecular species composition of phosphatidylinositol from the brain, retina, liver and muscle of cod (Gadus morhua). Lipids, 25, 691-694 (1990).
Bezard,J., Ouedraogo,M.A. and Sempore,G. Stereospecific analysis of the palmito-oleo-linolein of cottonseed oil. Rev. Franc. Corps Gras, 37, 171-175 (1990).
Bezard,J., Ouedraogo,M.A., Sempore,G. and Schreiber,L. Study of the stereospecific distribution of fatty acids in the triglycerides of cottonseed oil. Rev. Franc. Corps Gras, 37, 83-90 (1990).
Biesalski,H.K. Separation of retinyl esters and their geometric isomers by isocratic adsorption HPLC. Methods Enzymol., 189, 181-189 (1990).
Blair,I.A. Electron-capture negative-ion chemical ionization MS of lipid mediators Methods Enzymol., 187, 13-23 (1990).
Blank,M.L., Cress,E.A., Fitzgerald,V. and Snyder,F. TLC and HPLC separation of glycerolipid subclasses as benzoates. Derivatives of ether and ester analogues of phosphatidylcholine, phosphatidylethanolamine and platelet activating factor. J. Chromatogr. A, 508, 382-385 (1990).
Blee,E. and Schuber,F. Stereochemistry of the epoxygenation of fatty acids catalyzed by soybean peroxygenase. Biochem. Biophys. Res. Commun., 173, 1354-1360 (1990).
Blunk,H.-C. and Steinhart,H. Separation of phospholipids in bovine tissue with disposable silica gel extraction columns. Z. Lebensm.-Unters. Forsch., 190, 123-125 (1990).
Bonnet,M., Denoyer,C. and Renou,J.P. High resolution 13C-NMR of rendered animal fats: degree of saturation of fatty acid chains and position on glycerol. Int. J. Food Sci. Technol., 25, 399-408 (1990).
Borgeat,P., Picard,S., Vallerand,P., Bourgoin,S., Odeimat,A., Sirois,P. and Poubelle,P.E. Automated on-line extraction and profiling of lipoxygenase products of arachidonic acid by HPLC. Methods Enzymol., 187, 98-116 (1990).
Bortolomeazzi,R., Frega,N. and Lercker,G. Rapid determination of free and esterified sterols using prepacked silica columns. Ital. J. Food Sci., 2, 265-268 (1990).
Boyle,L.E., Sklar,L.A. and Traynor-Kaplan,A.E. An HPLC procedure for separating polyphosphoinositides on hydroxylapatite. J. Lipid Res., 31, 157-159 (1990).
Bradamante,S., Barchiesi,E. Barenghi,L. and Zoppi,F. An alternative expeditious analysis of phospholipid composition in human blood plasma by 31P NMR spectroscopy. Anal. Biochem., 185, 299-303 (1990).
Bradova,V., Smid,F., Ledvinova,J. and Michalec,C. Improved one-dimensional TLC for the separation of phospholipids in biological materials. J. Chromatogr. B, 533, 297-299 (1990).
Brash,A.R. and Hawkins,D.J. HPLC for chiral analysis of eicosenoids. Methods Enzymol., 187, 187-195 (1990).
Brooks,C.J.W., Cole,W.J. and Anderson,R.A. Analytical GC separation of diastereomeric tert.-butylmethoxyphenylsilyl ethers. J. Chromatogr. A, 514, 305-308 (1990).
Butikofer,P., Kuypers,F.A., Shackleton,C., Brodbeck,U. and Stieger,S. Molecular species analysis of the glycosylphosphatidylinositol anchor of Torpedo marmorata acetylcholinesterase. J. Biol. Chem., 265, 18983-18987 (1990).
Camacho,P.L., Geiger,E., Vigh,G., Webster,R. and Thompson,D.H. Separation of the enantiomeric intermediates of some platelet-activating factor analogues on a naphthylalanine-type Pirkle column. J. Chromatogr. A, 506, 611-616 (1990).
Cambron,L.D. and Leskawa,K.C. A sensitive method to quantitate gangliosides of the gangliotetraose series directly in chromatograms using peroxidase conjugated cholera toxin. Stain Technol., 65, 293-297 (1990).
Cantafora,A., Cardelli,M. and Masella,R. Separation and determination of molecular species of phosphatidylcholines in biological samples by HPLC. J. Chromatogr. A, 507, 339-349 (1990).
Carballeira,N.M. and Reyes,E.D. Identification of the new 23-methyl-5,9-pentacosadienoic acid in the sponge Cribrochalina vasculum. Lipids, 25, 69-71 (1990).
Carballeira,N.M. and Shalabi,F. Identification of naturally occurring trans,trans 5,9 fatty acids from the sponge Plakortis halichondroides. Lipids, 25, 835-840 (1990).
Carlson,K.D., Chaudhry,A., Peterson,R.E. and Bagby,M.O. Preparative chromatographic isolation of hydroxy acids from Lesquerella fendleri and L. gordonii seed oils. J. Am. Oil Chem. Soc., 67, 495-498 (1990).
Catella,F. and Fitzgerald,G.A. Measurement of thromboxane metabolites by GC-MS. Methods Enzymol., 187, 42-50 (1990).
Chaves das Neves,H.J., Vasconcelos,A.M.P. and Vasconcelos,O. A simple and rapid method for the study of triglyceride fatty acid profiles in human serum by capillary GC. J. High Resolut. Chromatogr., 13, 520-522 (1990).
Chen,S., Kirschner,G. and Benefenati,E. Quantitative analysis of 1-stearoyl-2-oleoyl-sn-glycero-3-phosphoserine by negative ion fast-atom bombardment mass spectrometry. Rapid Commun. Mass Spectrom., 4, 214-216 (1990).
Chen,S., Kirschner,G. and Traldi,P. Positive FAB-MS analysis of the molecular species of glycerophosphatidylserine. Anal. Biochem., 191, 100-105 (1990).
Chen,S., Mariot,R., Kirschner,G., Favretto,D. and Traldi,P. Analysis of arachidonic acid-containing molecular species in glycerophospholipid classes from rat kidney by fast atom bombardment MS. Rapid Commun. Mass Spectrom., 4, 495-497 (1990).
Cheung,A.P. and Olson,L.L. 1H-NMR assay of phosphatidylcholine and phosphatidylethanolamine in AL721. J. Pharm. Biomed. Anal., 8, 729-734 (1990).
Chilton,F.H. Separation and characterization of arachidonate-containing phospholipids. Methods Enzymol., 187, 157-167 (1990).
Christensen,S. and Harbak,H. Serial separation of inositol phosphates including pentakis- and hexakisphosphates on small ion exchange columns. J. Chromatogr. B, 533, 201-206 (1990).
Christie,W.W. Silver ion chromatography of triacylglycerols on solid phase extraction columns packed with a bonded sulphonic acid phase. J. Sci. Food Agric., 52, 573-577 (1990).
Clay,K.L. Quantitation of platelet-activating factor by GC-MS Methods Enzymol., 187, 134-142 (1990).
Coene,I., Ramos,M.E., Van den Eeckhout,E., Sandra,P. and van den Bossche,W. Evaluation of densitometric quantitation of ether phospholipids by HP TLC. Chromatographia, 30, 414-420 (1990).
Colarow,L. Quantitative transmittance densitometry of phospholipids after their specific detection with a molybdate reagent on silica gel plates. J. Planar Chromatogr., 3, 228-231 (1990).
Colarow,L. Quantitation of ceramides with essential fatty acid moieties in the human skin surface and blood plasma lipids. J. Planar Chromatogr. - Mod. TLC, 3, 126-132 (1990).
Costello,C.E. and Vath,J.E. Tandem mass spectrometry of glycolipids. Methods Enzymol., 193, 738-771 (1990).
Crockett, J.S., Gross, M.L., Christie, W.W. and Holman, R.T. Collisional activation of a series of homoconjugated octadecadienoic acids with fast atom bombardment and tandem mass-spectrometry. J. Am. Soci. Mass Spectrom., 1, 183-191 (1990); DOI.
Dabrowski,U., Dabrowski,J., Helling,F. and Wiegandt,H. Novel-phosphorus-containing glycosphingolipids from the blowfly Calliphora vivina Meigen. Structural analysis by 1H and 1H[31P]-edited NMR spectroscopy at 600 and 500 MHz. J. Biol. Chem., 265, 9737-9743 (1990).
DaTorre,S.D., Corr,P.B. and Creer,M.H. A sensitive method for the quantification of the mass of inositol phosphates using GC-MS. J. Lipid Res., 31, 1925-1934 (1990).
Dawson,M. and McGee,C. Comparison between ethanol and methanol for the reversed-phase HPLC analysis of leukotriene B4 and its metabolites in cell incubation supernatants. J. Chromatogr. B, 532, 379-386 (1990).
De Jong,C. and Badings,H.T. Determination of free fatty acids in milk and cheese. Procedures for extraction, clean up and capillary GC analysis. J. High Resolut. Chromatogr., 13, 94-98 (1990).
De Leenheer,A.P. and Lambert,W.E. MS of methyl ester of retinoic acid. Methods Enzymol., 189, 104-111 (1990).
de Sousa,C., English,N.R., Stacey,T.E. and Chalmers,R.A. Measurement of L-carnitine and acylcarnitines in body fluids and tissues in children and in adults. Clin. Chim. Acta, 187, 317-328 (1990).
DeLuca,S., Sarver,E.W., Harrington,P.D. and Voorhees,K.J. Direct analysis of bacterial fatty acids by Curie-Point pyrolysis tandem MS. Anal. Chem., 62, 1465-1472 (1990).
Demirbuker,M. and Blomberg,L.G. Group separation of triacylglycerols on micropacked argentation columns using supercritical media as mobile phases. J. Chromatogr. Sci., 28, 67-72 (1990).
Diczfalusy,U., Alexson,S.E.H., Sisfontes,L., Olund,J. and Bjorkhem,A. Identification of intermediates in the peroxisomal beta-oxidation of linoleic acid. Biochim. Biophys. Acta, 1043, 182-188 (1990).
Dobmeyer,D.J., Corr,P.B. and Creer,M.H. A sensitive radiometric assay for lysophosphatidylcholine. Anal. Biochem., 185, 36-43 (1990).
Doehl,J. and Greibrokk,T. Determination of prostaglandins in human seminal fluid by solid-phase extraction, pyridinium dichromate derivatization and HPLC. J. Chromatogr. B, 529, 21-32 (1990).
Domon,B., Vath,J.E. and Costello,C.E. Analysis of derivatised ceramides and neutral glycosphingolipids by high-performance tandem mass spectrometry. Anal. Biochem., 184, 151-164 (1990).
Douce,R., Joyard,J., Block,M.A, and Dorne,A.-J. Glycolipid analyses and synthesis in plastids. In: Methods in Plant Biochemistry 4. Lipids, Membranes and Aspects of Photobiology. pp. 71-103 (ed. J.L. Harwood & J.R. Bowyer, Academic Press, London) (1990).
Doumenq,P., Guiliano,M., Bertrand,J.C. and Mille,G. GC/FTIR analysis of fatty acid methyl esters. Appl. Spect., 44, 1355-1359 (1990).
Dworzanski,J.P., Berwlad,L. and Meuzelaar,H.L.C. Pyrolytic methylation-gas chromatography of whole bacterial cells for rapid profiling of cellular fatty acids. Appl. Environm. Microbiol., 56, 1717-1724 (1990).
Eble,K.S., Coleman,W.B., Hantgan,R.R. and Cunningham,C.C. Tightly associated cardiolipin in the bovine heart mitochondrial ATP synthase as analyzed by 31P NMR spectroscopy. J. Biol. Chem., 265, 19434-19440 (1990).
Eichenberger,W. Identification of new plant lipids: structure of a second betaine lipid from algae. In: 'Plant Lipid Biochemistry, Structure and Utilization', pp. 9-16 (edited by P.J. Quinn & J.L. Harwood, Portland Press, London) (1990).
Engel,K-H, Albrecht,W. and Heidlas,J. Enantiodifferentiation of gamma- and delta-lactones by GC separation of diastereomeric carbamoyloxy carboxamide derivatives. J. Agric. Food Chem., 38, 244-247 (1990).
Federici,F., Lionetti,P., Messina,A., Nicoletti,I. and Sinibaldi,M. HPLC separation of phospholipids on cobalt(III) complex bonded silica gel. Anal. Letts., 23, 1265-1277 (1990).
Fischer,C. and Holl,G. Lipoprotein lipase as a new tool in steryl ester analysis. Lipids, 25, 292-295 (1990).
Fourneron,J.-D., Chiche,M. and Pieroni,G. Stereoselective lipase-catalysed acylation of terpenic allylic alcohols by fatty acid anhydrides. Tetrahedron Letts., 31, 4875-4878 (1990).
Frankel,E.N., Neff,W.E. and Miyashita,K. Autoxidation of polyunsaturated triacylglycerols. II. Trilinolenoylglycerol. Lipids, 25, 40-47 (1990).
Frankel,E.N., Neff,W.E. and Weisleder,D. Determination of methyl linoleate hydroperoxides by 13C NMR. Methods Enzymol., 186, 380-387 (1990).
Furr,H.C. Reversed-phase HPLC of retinyl esters. Methods Enzymol., 189, 85-94 (1990).
Gandini,C., Kitsos,M., Massolini,G., De Lorenzi,E., Soldi,A., Caccialanza,G. and Kirschner,G. Determination of gangliosides in parental dosage form by HPLC. J. Pharm. Biomed. Anal., 8, 1063-1066 (1990).
Gelpi,E. and Abian,J. Comparative evaluation of combined HPLC-MS and GC-MS methods for the study of eicosanoid metabolism. LC-GC Int., Vol. 3. No. 12, pp. 30-38 (1990).
German,J.B. and Berger,R. Formation of 8,15-dihydroxy eicosatetraenoic acid via 15- and 12-lipoxygenases in fish gill. Lipids, 25, 849-853 (1990).
Glass,R.L. Separation of phosphatidylcholine and its molecular species by HPLC. J. Agric. Food Chem., 38, 1684-1686 (1990).
Goldman,H.D., Hsu,F.F. and Sherman,W.R., Studies of the permethylation/dephosphorylation of inositol polyphosphates: an approach to a more sensitive assay. Biomed. Environm. Mass Spectrom., 19, 771-776 (1990).
Graff,G., Anderson,L.A. and Jaques,L.W., Preparation and purification of soybean lipoxygenase-derived unsaturated hydroperoxy and hydroxy fatty acids and determination of molar absorptivities of hydroxy fatty acids. Anal. Biochem., 188, 38-47 (1990).
Graff,G., Anderson,L.A., Jaques,L.W. and Scannell,R.T., Evidence for the formation of 2-hydroxyethyl esters by action of fatty acids with diazomethane in diethyl ether. Chem. Phys. Lipids, 53, 27-36 (1990).
Grob,K., Lanfranchi,M. and Mariani,C., Evaluation of olive oils through the fatty alcohols, the sterols and their esters by coupled LC-GC. J. Am. Oil Chem. Soc., 67, 626-634 (1990).
Gunstone,F.D. 13C-NMR spectra of some synthetic glycerol esters alone or as mixtures. Chem. Phys. Lipids, 56, 195-199 (1990).
Gunstone,F.D. 13C-NMR spectra of oils containing gamma linolenic acid. Chem. Phys. Lipids, 56, 201-207 (1990).
Gunstone,F.D. 1H- and 13C-NMR spectra of six n-3 polyene esters. Chem. Phys. Lipids, 56, 227-229 (1990).
Haalck,L. and Spener,F., Prediction of retention times of hydroxylated triacylglycerols in reversed-phase HPLC. J. Chromatogr. A, 498, 410-413 (1990).
Hack,M.H. and Helmy,F.M., TLC analysis of myelin lipids, their differential O-deacylation by primary alkylamines and their selective staining by thionine. A limited phylogenic study. J. Chromatogr. B, 525, 339-348 (1990).
Hanahan,D.J., Isolation of platelet-activating factor and purification by TLC. Methods Enzymol., 187, 152-157 (1990).
Hanahan,D.J., Nouchi,T., Weintraub,S.T. and Olson,M.S., Novel route to preparation of high purity lysoplasmenylethanolamine. J. Lipid Res., 31, 2113-2117 (1990).
Harvey,D.J. Pyridine-containing derivatives for the structural elucidation of the alkyl chains of lipids by MS and a comparison with the spectra of related heterocyclic derivatives. Spectros. Int. J., 8, 211-244 (1990).
Hashimoto,A. and Ichimoto,I., (S)-3-Acetyl-1,2-diacyl-sn-glycerols from the lipids of Drosicha corpulenta Kuwana (Homoptera: Margarodidae). Appl. Entomol. Zool., 25, 515-516 (1990).
Hayashi,A., Matsubara,T., Nakamura,T. and Kinoshita,T., Structure determination of phosphonosphingolipids by FAB and tandem MS. Chem. Phys. Lipids, 52, 57-67 (1990).
Hayashi,A., Mishima,Y. and Matsubara,T., Occurrence and structure determination of octadecasphinga-4,8,10-trienine. Chem. Phys. Lipids, 52, 171-178 (1990).
Hayashi,H., Adachi,H., Kataoka,K., Sato,H. and Akino,T., Molecular species profiles of acidic phospholipids in lung fractions of adult and perinatal rabbits. Biochim. Biophys. Acta, 1042, 126-131 (1990).
Herman,J.A. and Shafer,K.H., Bioanalytical application of TLC/FTIR. Chem. Anal. (N.Y.), 108, 157-166 (1990).
Herslof,B., Olsson,U. and Tingvall,P. Characterization of lecithins and phospholipids by HPLC with light scattering detection. In: 'Phospholipids', pp. 295-298 (eds I. Hanin & G. Pepeu, Plenum Press, New York) (1990).
Higashidate,S., Yamauchi,Y. and Saito,M., Enrichment of eicosapentaenoic acid and docosahexaenoic acid esters from esterified fish oil by programmed extraction - elution with supercritical carbon dioxide. J. Chromatogr. A, 515, 295-303 (1990).
Hirashima,Y., Farooqui,A.A., Murphy,E.J. and Horrocks,L.A., Purification of plasmalogens using Rhizopus delemar lipase and naja naja phospholipase A2. Lipids, 25, 344-348 (1990).
Hofmann,U., Holzer,S. and Meese,C.O., Pentafluorophenyldiazoalkanes as novel derivatization reagents for the determination of sensitive carboxylic acids by GC-negative-ionMS. J. Chromatogr. A, 508, 349-356 (1990).
Hofmann,U., Seefried,S., Meese,C.O., Mettang,T., Hubel,E. and Kuhlmann,U., Measurement of 12(S)-hydroxy-5Z,8E,10E-heptadecatrienoic acid and its metabolite 12-oxo-5Z,8E,10E-heptadecatrienoic acid in human plasma by GC/negative ion CI-MS. Anal. Biochem., 189, 244-248 (1990).
Holgersson,J., Jovall,P.-A., Samuelsson,B.E. and Breimer,B.E., Structural characterization of non-acid glycosphingolipids in kidneys of single blood group O and A pigs. J. Biochem. (Tokyo), 108, 766-777 (1990).
Holte,L.H., Van Kuijk,F.J.G.M. and Dratz,E.A. Preparative HPLC purification of polyunsaturated phospholipids and characterization using UV derivative spectroscopy. Anal. Biochem., 188, 136-141 (1990).
Horiike,M., Yuan,G. and Hirano,C. Location of double-bond position in tetradecenols without chemical modification by MS. Org. Mass Spectrom., 25, 329-332 (1990).
Husek,P., Rijks,J.A., Leclercq,P.A. and Cramers,C.A. Fast esterification of fatty acids with alkyl chloroformates. Optimization and application in GC. J. High Resolut. Chromatogr., 13, 633-638 (1990).
Husmann,H., Schomburg,G., Mueller,K.D., Nalik,H.P. and Von Recklinghausen,G. GC fatty acid methyl ester analysis for characterization of bacteria: formation of aldehydes from 3-hydroxy fatty acid methyl esters during sample introduction. J. High Resolut. Chromatogr., 13, 780-782 (1990).
Huwyler,J. and Gut,J. Single-step extraction of leukotrienes and related compounds and their simultaneous analysis by HPLC. Anal. Biochem., 188, 374-382 (1990).
Ioneda,T. O-Benzoylation as a derivatization procedure for analysis of 1-monomycolylglycerol by MS. Chem. Phys. Lipids, 53, 357-360 (1990).
Ioneda,T. Mass spectrometric analysis of O-peracetylated derivatives of 1-monomycolylglycerol isolated from Corynebacterium pseudotuberculosis, Rhodococcus rhodochrous and R.lentifragmentus. Chem. Phys. Lipids, 54, 215-220 (1990).
Irie,A., Kubo,H. and Hoshi,M. Glucosylceramide having a novel tri-unsaturated long-chain base from the spermatozoa of the starfish, Asterias amurensis. J. Biochem. (Tokyo), 107, 578-586 (1990).
Irie,A., Kubo,H., Inagaki,F. and Hoshi,M. Ceramide dihexosides from the spermatozoa of the starfish, Asterias amurensis, consist of gentiobiosyl-, cellobiosyl- and lactosyl-ceramide. J. Biochem. (Tokyo), 108, 531-536 (1990).
Irvine,R.F. (editor) 'Methods in Inositide Research', Raven Press, New York (1990).
Itabashi,Y., Kuksis,A. and Myher,J.J. Determination of molecular species of enantiomeric diacylglycerols by chiral phase HPLC and polar capillary GC. J. Lipid Res., 31, 2119-2126 (1990).
Itabashi,Y., Kuksis,A., Marai,L. and Takagi,T. HPLC resolution of diacylglycerol moieties of natural triacylglycerols on a chiral phase consisting of bonded R-(+)-1-(1-naphthyl)-ethylamine. J. Lipid Res., 31, 1711-1717 (1990).
Janero,D.R. and Burghardt,C. Solid-phase extraction on silica cartridges as an aid to platelet-activating factor enrichment and analysis. J. Chromatogr. B, 526, 11-24 (1990).
Jensen,N., Lam,K., Cody,R.B. and Tamura,J. Evidence for distinction of cis and trans isomers of mono-unsaturated fatty acids by FAB-MS. Rapid Commun. Mass Spectrom., 4, 239-241 (1990).
Jeong,B.Y., Ohshima,T. and Koizumi,C. Molecular species of 1-O-alk-1-enyl-2-acyl-, 1-O-alkyl-2-acyl- and 1,2-diacyl glycerophospholipids in Japanese oyster, Crassostrea gigas (Thunberg). Lipids, 25, 624-632 (1990).
Jiao,S., Cole,T.G., Kitchens,R.T., Pfleger,B. and Schonfeld,G. Genetic heterogeneity of lipoproteins in inbred strains of mice: analysis by gel-permeation chromatography. Metabolism, 39, 155-160 (1990).
Johnson,S.W., Masserini,M. and Alhadeff,J.A. HPLC analysis of fucoganglioside hydrolysis by alpha-L-fucosidase. Anal. Biochem., 189, 209-212 (1990).
Juaneda,P., Rocquelin,G. and Astorg,P.O. Separation and quantification of heart and liver phospholipid classes by HPLC using a light-scattering detector. Lipids, 25, 756-759 (1990).
Judge,D.N., Mullins,D.E. and Eaton,J.L. Microquantity analysis of insect hemolymph lipids by HP-TLC. J. Planar Chromatogr. - Mod. TLC, 2, 442-446 (1990).
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© Data compiled by Bill Christie
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