Highlights from the Lipid Analysis Literature - 2016
The following references were collected as part of a weekly literature search that reflects my (former) personal research interests. However, most mainstream lipid analytical topics are covered. Among the exceptions are "steroidal hormones", "prostanoids", "fat-soluble vitamins" and "terpenoids", although some papers in these categories may be posted. My intention is to list only those papers that exhibit novel analytical methodology as opposed to tried and tested methods, although this may appear to introduce a bias towards modern mass spectrometry techniques. References are listed alphabetically by the first author.
- Abbassi-Ghadi, N., Jones, E.A., Gomez-Romero, M., Golf, O., Kumar, S., Huang, J.Z., Kudo, H., Goldin, R.D., Hanna, G.B. and Takats, Z. A comparison of DESI-MS and LC-MS for the lipidomic profiling of human cancer tissue. J. Am. Soc. Mass Spectrom., 27, 255-264 (2016); DOI.
- Al Makdessi, S., Sweidan, H., Schmid, E., Weimar, U., Gulbins, E. and Lang, F. Quantitative determination of ceramide molecular species in dendritic cells. Cell. Physiol. Biochem., 39, 1608-1617 (2016); DOI.
- Al Masoud, N., Correa, E., Trivedi, D.K. and Goodacre, R. Fractional factorial design of MALDI-TOF-MS sample preparations for the optimized detection of phospholipids and acylglycerols. Anal. Chem., 88, 6301-6308 (2016); DOI.
- Al Masoud, N., Xu, Y., Trivedi, D.K., Salivo, S., Abban, T., Rattray, N.J.W., Szula, E., Al Rabiah, H., Sayqal, A. and Goodacre, R. Classification of Bacillus and Brevibacillus species using rapid analysis of lipids by mass spectrometry. Anal. Bioanal. Chem., 408, 7865-7878 (2016); DOI.
- Albrecht, S., Vainauskas, S., Stockmann, H., McManus, C., Taron, C.H. and Rudd, P.M. Comprehensive profiling of glycosphingolipid glycans using a novel broad specificity endoglycoceramidase in a high-throughput workflow. Anal. Chem., 88, 4795-4802 (2016);DOI.
- Aleman-Nava, G.S., Cuellar-Bermudez, S.P., Cuaresma, M., Bosma, R., Muylaert, K., Ritmann, B.E. and Parra, R. How to use Nile Red, a selective fluorescent stain for microalgal neutral lipids. J. Microbiol. Methods, 128, 74-79 (2016); DOI.
- Almostafa, M., Allehyane, B., Egli, S., Bottaro, C., Fridgen, T.D. and Banoub, J. Tandem mass spectrometry determination of the putative structure of a heterogeneous mixture of Lipid A(s) isolated from the lipopolysaccharide of the Gram-negative bacteria Aeromonas liquefaciens SJ-19a. Rapid Commun. Mass Spectrom., 30, 1043-1058 (2016); DOI.
- Araujo, P., Tilahun, E., Breivik, J.F., Abdulkader, B.M., Froyland, L. and Zeng, Y.X. A simple liquid extraction protocol for overcoming the ion suppression of triacylglycerols by phospholipids in liquid chromatography mass spectrometry studies. Talanta, 148, 463-471 (2016); DOI.
- Arnardottir, H., Orr, S.K., Dalli, J. and Serhan, C.N. Human milk proresolving mediators stimulate resolution of acute inflammation. Mucosal Immunol., 9, 757-766 (2016); DOI.
- Atila, M., Katselis, G., Chumala, P. and Luo, Y. Characterization of N-succinylation of L-lysylphosphatidylglycerol in Bacillus subtilis using tandem mass spectrometry. J. Am. Soc. Mass Spectrom., 27, 1606-1613 (2016); DOI.
- Baba, T., Campbell, J.L., Le Blanc, J.C.Y. and Baker, P.R.S. In-depth sphingomyelin characterization using electron impact excitation of ions from organics and mass spectrometry. J. Lipid Res., 57, 858-867 (2016); DOI.
- Baba, T., Campbell, J.L., Le Blanc, J.C.Y. and Baker, P.R.S. Structural identification of triacylglycerol isomers using electron impact excitation of ions from organics (EIEIO). J. Lipid Res., 57, 2015-2027 (2016); DOI.
- Balas, L., Bertrand-Michel, J., Viars, F., Faugere, J., Lefort, C., Caspar-Bauguil, S., Langin, D. and Durand, T. Regiocontrolled syntheses of FAHFAs and LC-MS/MS differentiation of regioisomers. Org. Biomol. Chem., 14, 9012-9020 (2016); DOI.
- Balsgart, N.M., Mulbjerg, M., Guo, Z., Bertelsen, K. and Vosegaard, T. High throughput identification and quantification of phospholipids in complex mixtures. Anal. Chem., 88, 2170-2176 (2016); DOI.
- Bansal, S. and Durrett, T.P. Rapid quantification of low-viscosity acetyl-triacylglycerols using electrospray ionization mass spectrometry. Lipids, 51, 1093-1102 (2016); DOI.
- Barden, A.E., Moghaddami, M., Mas, E., Phillips, M., Cleland, L.G. and Mori, T.A. Specialised pro-resolving mediators of inflammation in inflammatory arthritis. PLEFA, 107, 24-29 (2016); DOI.
- Barry, K.M., Dinan, T.G., Murray, B.A. and Kelly, P.M. Comparison of dairy phospholipid preparative extraction protocols in combination with analysis by high performance liquid chromatography coupled to a charged aerosol detector. Int. Dairy J., 56, 179-185 (2016); DOI.
- Bartosinska, E., Buszewska-Forajta, M. and Siluk, D. GC-MS and LC-MS approaches for determination of tocopherols and tocotrienols in biological and food matrices. J. Pharm. Biomed. Anal., 127, 156-169 (2016); DOI.
- Basit, A., Pontis, S., Piomelli, D. and Armirotti, A. Ion mobility mass spectrometry enhances low-abundance species detection in untargeted lipidomics. Metabolomics, 12, 50 (2016); DOI.
- Bauersachs, T. and Schwark, L. Glycerol monoalkanediol diethers: a novel series of archaeal lipids detected in hydrothermal environments. Rapid Commun. Mass Spectrom., 30, 54-60 (2016); DOI.
- Behrens, B., Baune, M., Jungkeit, J., Tiso, T., Blank, L.M. and Hayen, H. High performance liquid chromatography-charged aerosol detection applying an inverse gradient for quantification of rhamnolipid biosurfactants. J. Chromatogr. A, 1455, 125-132 (2016); DOI.
- Behrens, B., Engelen, J., Tiso, T., Blank, L.M. and Hayen, H. Characterization of rhamnolipids by liquid chromatography/mass spectrometry after solid-phase extraction. Anal. Bioanal. Chem., 408, 2505-2514 (2016); DOI.
- Bian, Q.X., Wang, W.H., Wang, N.N., Peng, Y., Ma, W. and Dai, R.H. Quantification of arachidonic acid and its metabolites in rat tissues by UHPLC-MS/MS: application for the identification of potential biomarkers of benign prostatic hyperplasia. PLOS One, 11, e0166777 (2016); DOI.
- Bierhanzl, V.M., Bursova, M., Ston, M., Cabala, R. and Seydlova, G. Simultaneous analysis of polar and non-polar components of cell membrane phospholipids by GC-MS. Chem. Papers, 70, 1309-1315 (2016); DOI.
- Bierhanzl, V.M., Cabala, R., Ston, M., Kotora, P., Ferenczy, V., Blasko, J., Kubinec, R. and Seydlova, G. Direct injection mass spectrometry, thin layer chromatography, and gas chromatography of Bacillus subtilis phospholipids. Monats. Chem., 147, 1385-1391 (2016); DOI.
- Bilgin, M., Born, P., Fezza, F., Heimes, M., Mastrangelo, N., Wagner, N., Schultz, C., Maccarrone, M., Eaton, S., Nadler, A., Wilm, M. and Shevchenko, A. Lipid discovery by combinatorial screening and untargeted LC-MS/MS. Sci. Rep., 6, 27920 (2016); DOI.
- Bin, J., Ai, F.F., Fan, W., Zhou, J.H. and Zhang, Z.M. Rapid determination of unsaturated fatty acids in vegetable oil by raman spectroscopy and chemometrics. Anal. Letts, 49, 831-842 (2016); DOI.
- Boiten, W., Absalah, S., Vreeken, R., Bouwstra, J. and van Smeden, J. Quantitative analysis of ceramides using a novel lipidomics approach with three dimensional response modelling. Biochim. Biophys. Acta, 1861, 1652-1661 (2016); DOI.
- Boka, B., Manczinger, L., Kecskemeti, A., Chandrasekaran, M., Kadaikunnan, S., Alharbi, N.S., Vagvolgyi, C. and Szekeres, A. Ion trap mass spectrometry of surfactins produced by Bacillus subtilis SZMC6179J reveals novel fragmentation features of cyclic lipopeptides. Rapid Commun. Mass Spectrom., 30, 1581-1590 (2016); DOI.
- Bojic, L.A., McLaren, D.G., Harms, A.C., Hankemeier, T., Dane, A., Wang, S.P., Rosa, R., Previs, S.F., Johns, D.G. and Castro-Perez, J.M. Quantitative profiling of oxylipins in plasma and atherosclerotic plaques of hypercholesterolemic rabbits. Anal. Bioanal. Chem., 408, 97-105 (2016); DOI.
- Boughton, B.A., Thinagaran, D., Sarabia, D., Bacic, A. and Roessner, U. Mass spectrometry imaging for plant biology: a review. Phytochem. Rev., 15, 445-488 (2016); DOI.
- Bruhl, L., Weisshaar, R. and Matthaus, B. Epoxy fatty acids in used frying fats and oils, edible oils and chocolate and their formation in oils during heating. Eur. J. Lipid Sci. Technol., 118, 425-434 (2016); DOI.
- Buré, C., Cacas, J.L., Badoc, A., Mongrand, S. and Schmitter, J.M. Branched glycosylated inositolphosphosphingolipid structures in plants revealed by MS3 analysis. J. Mass Spectrom., 51, 305-308 (2016); DOI.
- Busta, L., Budke, J.M. and Jetter, R. Identification of beta-hydroxy fatty acid esters and primary, secondary-alkanediol esters in cuticular waxes of the moss Funaria hygrometrica. Phytochemistry, 121, 38-49 (2016); DOI.
- Byeon, S.K., Lee, J.C., Chung, B.C., Seo, H.S. and Moon, M.H. High-throughput and rapid quantification of lipids by nanoflow UPLC-ESI-MS/MS: application to the hepatic lipids of rabbits with nonalcoholic fatty liver disease. Anal. Bioanal. Chem., 408, 4975-4985 (2016); DOI.
- Byrdwell, W.C. The simulacrum system as a construct for mass spectrometry of triacylglycerols and others. Lipids, 51, 211-227 (2016); DOI.
- Bystricka, Z. and Durackova, Z Gas chromatography determination of fatty acids in the human erythrocyte membranes - A review. PLEFA, 115, 35-40 (2016); DOI.
- Cai, H.-H., Lin, L.-J., Ding, S.-W., Cui, X.-H. and Chen, Z. Fast quantification of fatty acid profile of intact fish by intermolecular double-quantum coherence 1H-NMR spectroscopy. Eur. J. Lipid Sci. Technol., 118, 1150-1159 (2016); DOI.
- Cajka, T. and Fiehn, O. Toward merging untargeted and targeted methods in mass spectrometry-based metabolomics and lipidomics. Anal. Chem., 88, 524-545 (2016); DOI.
- Cajka, T. and Fiehn, O. Increasing lipidomic coverage by selecting optimal mobile-phase modifiers in LC-MS of blood plasma. Metabolomics, 12, 34 (2016); DOI.
- Caligiani, A., Nocetti, M., Lolli, V., Marseglia, A. and Palla, G. Development of a quantitative GC-MS method for the detection of cyclopropane fatty acids in cheese as new molecular markers for Parmigiano Reggiano authentication. J. Agric. Food Chem., 64, 4158-4164 (2016); DOI.
- Camera, E., Ludovici, M., Tortorella, S., Sinagra, J.L., Capitanio, B., Goracci, L. and Picardo, M. Use of lipidomics to investigate sebum dysfunction in juvenile acne. J. Lipid Res., 57, 1051-1058 (2016); DOI.
- Canela, N., Herrero, P., Marine, S., Nadal, P., Ras, M.R., Rodriguez, M.A. and Arola, L. Analytical methods in sphingolipidomics: Quantitative and profiling approaches in food analysis. J. Chromatogr. A, 1428, 16-38 (2016); DOI.
- Canez, C.R., Shields, S.W.J., Bugno, M., Wasslen, K.V., Weinert, H.P., Willmore, W.G., Manthorpe, J.M. and Smith, J.C. Trimethylation enhancement using (13)C-diazomethane ((13)C- TrEnDi): increased sensitivity and selectivity of phosphatidylethanolamine, phosphatidylcholine, and phosphatidylserine lipids derived from complex biological samples. Anal. Chem., 88, 6996-7004 (2016); DOI.
- Cantley, A.M., Woznica, A., Beemelmanns, C., King, N. and Clardy, J. Isolation and synthesis of a bacterially produced inhibitor of rosette development in choanoflagellates. J. Am. Chem. Soc., 138, 4326-4329 (2016); DOI.
- Cao, Z.Y., Sun, L.H., Mou, R.X., Zhang, L.P., Lin, X.Y., Zhu, Z.W. and Chen, M.X. Profiling of phytohormones and their major metabolites in rice using binary solid-phase extraction and liquid chromatography-triple quadrupole mass spectrometry. J. Chromatogr. A, 1451, 67-74 (2016); DOI.
- Carballeira, N.M., Montano, N., Amador, L.A., Rodriguez, A.D., Golovko, M.Y., Golovko, S.A., Reguera, R.M., Alvarez-Velilla, R. and Balana-Fouce, R. Novel very long-chain alpha-methoxylated Delta 5,9 fatty acids from the sponge Asteropus niger are effective inhibitors of topoisomerases IB. Lipids, 51, 245-256 (2016); DOI.
- Cerutti-Delasalle, C., Mehiri, M., Cagliero, C., Rubiolo, P., Bicchi, C., Meierhenrich, U.J. and Baldovini, N. The (+)-cis- and (+)-trans-olibanic acids: key odorants of frankincense. Angew. Chem.-Int. Ed., 55, 13719-13723 (2016); DOI.
- Cha, E., Lee, K.M., Park, K.D., Park, K.S., Lee, K.W., Kim, S.M. and Lee, J. hydroxycholesterol levels in the serum and cerebrospinal fluid of patients with neuromyelitis optica revealed by LC-Ag+CIS/MS/MS and LC-ESI/MS/MS with picolinic derivatization: increased levels and association with disability during acute attack. PLoS One, 11, e0167819 (2016); DOI.
- Chang, K.J.L., Dunstan, G.A., Mansour, M.P., Jameson, I.D. and Nichols, P.D. A novel series of C-18-C-22 trans omega 3 PUFA from Northern and Southern Hemisphere strains of the marine haptophyte Imantonia rotunda. J. Applied Phycol., 28, 3363-3370 (2016); DOI.
- Chen, E., Kiebish, M.A., McDaniel, J., Gao, F., Narain, N.R., Sarangarajan, R., Kacso, G., Ravasz, D., Seyfried, T.N., Adam-Vizi, V. and Chinopoulos, C. The total and mitochondrial lipidome of Artemia franciscana encysted embryos. Biochim. Biophys. Acta, 1861, 1727-1735 (2016); DOI.
- Chen, J.Z., Green, K.B. and Nichols, K.K. Compositional analysis of wax esters in human meibomian gland secretions by direct infusion electrospray ionization mass spectrometry. Lipids, 51, 1269-1287 (2016); DOI.
- Chen, Y.C., Tsai, C.J. and Feng, C.H. Fluorescent derivatization combined with aqueous solvent-based dispersive liquid-liquid microextraction for determination of butyrobetaine, L-carnitine and acetyl-L-carnitine in human plasma. J. Chromatogr. A, 1464, 32-41 (2016); DOI.
- Chinta, S.P., Goller, S., Uhl, G. and Schulz, S. Identification and synthesis of branched wax-type esters, novel surface lipids from the spider Argyrodes elevatus (Araneae: Theridiidae). Chem. Biodiv., 13, 1202-1220 (2016); DOI.
- Christinat, N., Morin-Rivron, D. and Masoodi, M. High-throughput quantitative lipidomics analysis of nonesterified fatty acids in human plasma. J. Proteome Res., 15, 2228-2235 (2016); DOI.
- Chvalova, D. and Spicka, J. Identification of furan fatty acids in the lipids of common carp (Cyprinus carpio L.). Food Chem., 200, 183-188 (2016); DOI.
- Cífková, E., Hájek, R., Lísa, M. and Holcapek, M. Hydrophilic interaction liquid chromatography-mass spectrometry of (lyso)phosphatidic acids, (lyso)phosphatidylserines and other lipid classes. J. Chromatogr. A, 1439, 65-73 (2016); DOI.
- Ciucanu, I., Pilat, L., Ciucanu, C.I., Sisu, E. and Dumitrascu, V Simultaneous analysis of neutral monosaccharides, fatty acids and cholesterol as biomarkers from a drop of blood. Bioanalysis, 8, 2147-2156 (2016); DOI.
- Company-Arumi, D., Figueras, M., Salvado, V., Molinas, M., Serra, O. and Antico, E. The identification and quantification of suberin monomers of root and tuber periderm from potato (Solanum tuberosum) as fatty acyl tert-butyldimethylsilyl derivatives. Phytochem. Anal., 27, 326-335 (2016); DOI.
- Cossignani, L., Montesano, D., Simonetti, M.S. and Blasi, F. Authentication of Coffea arabica according to triacylglycerol stereospecific composition. J. Anal. Chem., 7482620 (2016); DOI.
- Couto, D., Melo, T., Maciel, E., Campos, A., Alves, E., Guedes, S., Domingues, M.R.M. and Domingues, P. New insights on non-enzymatic oxidation of ganglioside GM1 using mass spectrometry. J. Am. Soc. Mass Spectrom., 27, 1965-1978 (2016); DOI.
- Cruz, M., Wang, M., Frisch-Daiello, J. and Han, X. Improved butanol-methanol (BUME) method by replacing acetic acid for lipid extraction of biological samples. Lipids, 51, 887-896 (2016); DOI.
- Cutignano, A., Luongo, E., Nuzzo, G., Pagano, D., Manzo, E., Sardo, A. and Fontana, A. Profiling of complex lipids in marine microalgae by UHPLC/tandem mass spectrometry. Algal Res.-Biomass Biofuels Bioproducts, 17, 348-358 (2016); DOI.
- da Costa, E., Silva, J., Mendonça, S.H., Abreu, M.H. and Domingues, M.R. Lipidomic approaches towards deciphering glycolipids from microalgae as a reservoir of bioactive lipids. Marine Drugs, 14, 101 (2016); DOI.
- Delmonte, P. Evaluation of poly(90% biscyanopropyl/10% cyanopropylphenyl siloxane) capillary columns for the gas chromatographic quantification of trans fatty acids in non-hydrogenated vegetable oils. J. Chromatogr. A, 1460, 160-172 (2016); DOI.
- Delosiere, M., Sante-Lhoutellier, V., Chantelauze, C., Durand, D., Thomas, A., Joly, C., Pujos-Guillot, E., Remond, D., Comte, B., Gladine, C., Guy, A., Durand, T., Laurentie, M. and Dufour, C. Quantification of 4-hydroxy-2-nonenal-protein adducts in the in vivo gastric digesta of mini-pigs using a GC-MS/MS method with accuracy profile validation. Food Function, 7, 3497-3504 (2016); DOI.
- Demarque, D.P., Crotti, A.E.M., Vessecchi, R., Lopes, J.L.C. and Lopes, N.P. Fragmentation reactions using electrospray ionization mass spectrometry: an important tool for the structural elucidation and characterization of synthetic and natural products. Nat. Prod. Rep., 33, 432-455 (2016); DOI.
- Deng, P., Zhong, D.F., Wang, X., Dai, Y.L., Zhou, L., Leng, Y. and Chen, X.Y. Analysis of diacylglycerols by ultra performance liquid chromatography-quadrupole time-of-flight mass spectrometry: Double bond location and isomers separation. Anal. Chim. Acta, 925, 23-33 (2016); DOI.
- Dhanarajan, G., Rangarajan, V., Sridhar, P.R. and Sen, R. Development and scale-up of an efficient and green process for HPLC purification of antimicrobial homologues of commercially important microbial lipopeptides. ACS Sustain. Chem. Engin., 4, 6638-6646 (2016); DOI.
- Difusa, A., Mohanty, K. and Goud, V.V. The chemometric approach applied to FTIR spectral data for the analysis of lipid content in microalgae cultivated in different nitrogen sources. Biomass Conv. Bioref., 6, 427-433 (2016); DOI.
- Ding, S., Schwab, V.F., Ueberschaar, N., Roth, V.N., Lange, M., Xu, Y.P., Gleixner, G. and Pohnert, G. Identification of novel 7-methyl and cyclopentanyl branched glycerol dialkyl glycerol tetraethers in lake sediments. Org. Geochem., 102, 52-58 (2016); DOI.
- Divito, E.B., Kroniser, K.M. and Cascio, M. Multidimensional liquid chromatography coupled with tandem mass spectrometry for identification of bioactive fatty acyl derivatives. Front. Physiol., 7, 608 (2016); DOI.
- Donot, F., Strub, C., Fontana, A., Jouy, N., Delbes, C., Gunata, Z. and Schorr-Galindo, S. Rapid analysis and quantification of major neutral lipid species and free fatty acids by HPLC-ELSD from microalgae. Eur. J. Lipid Sci. Technol., 118, 1550-1556 (2016); DOI.
- Doomun, S.N.E., Loke, S., O'Callaghan, S. and Callahan, D.L. A simple method for measuring carbon-13 fatty acid enrichment in the major lipid classes of microalgae using GC-MS. Metabolites, 6, 42 (2016); DOI.
- Dorow, J., Becker, S., Kortz, L., Thiery, J., Hauschildt, S. and Ceglarek, U. Preanalytical investigation of polyunsaturated fatty acids and eicosanoids in human plasma by liquid chromatography-tandem mass spectrometry. Biopreserv. Biobank., 14, 107-113 (2016); DOI.
- dos Santos, F.N., Santos, J.M., Mesquita, .PR.R., Oliveira, K.B., Rodrigues, F.M., Lopes, W.A. and Eberlin, M.N. Immediate differentiation of unusual seed oils by easy ambient sonic-spray ionization mass spectrometry and chemometric analysis. Anal. Methods, 8, 3681-3690 (2016); DOI.
- Drechsler, R., Chen, S.W., Dancy, B.C.R., Mehrabkhani, L. and Olsen, C.P. HPLC-based mass spectrometry characterizes the phospholipid alterations in ether-linked lipid deficiency models following oxidative stress. PLOS One, 11, e0167229 (2016); DOI.
- Dufresne, M., Masson, J.F. and Chaurand, P. Sodium-doped gold-assisted laser desorption ionization for enhanced imaging mass spectrometry of triacylglycerols from thin tissue sections. Anal. Chem., 88, 6018-6025 (2016); DOI.
- Dupuy, A., Le Faouder, P., Vigor, C., Oger, C., Galano, J.M., Dray, C., Lee, J.C.Y., Valet, P., Gladine, C., Durand, T. and Bertrand-Michel, J. Simultaneous quantitative profiling of 20 isoprostanoids from omega-3 and omega-6 polyunsaturated fatty acids by LC-MS/MS in various biological samples. Anal. Chim. Acta, 921, 46-58 (2016); DOI.
- Dzhatdoeva, A.A., Polimova, A.M., Proskurnina, E.V., Proskurnin, M.A. and Vladimirov, Y.A. Determination of lipids and their oxidation products by IR spectrometry. J. Anal. Chem., 71, 542-548 (2016); DOI.
- Ellis, S.R., Cappell, J., Potocnik, N.O., Balluff, B., Hamaide, J., Van der Linden, A. and Heeren, R.M.A. More from less: high-throughput dual polarity lipid imaging of biological tissues. Analyst, 141, 3832-3841 (2016); DOI.
- Englert, M., Ulms, K., Wendlinger, C. and Vetter, W. Isolation of a furan fatty acid from Hevea brasiliensis latex employing the combined use of pH-zone-refining and conventional countercurrent chromatography. J. Sep. Sci., 39, 490-495 (2016); DOI.
- Facchini, L., Losito, I., Cataldi, T.R.I. and Palmisano, F. Ceramide lipids in alive and thermally stressed mussels: an investigation by hydrophilic interaction liquid chromatography-electrospray ionization Fourier transform mass spectrometry. J. Mass Spectrom., 51, 768-781 (2016); DOI.
- Fan, H., Smuts, J., Bai, L., Walsh, P., Armstrong, D.W. and Schug, K.A. Gas chromatography-vacuum ultraviolet spectroscopy for analysis of fatty acid methyl esters. Food Chem., 194, 265-271 (2016); DOI.
- Fardin-Kia, A.R. Preparation, isolation and identification of non-conjugated C18:2 fatty acid isomers. Chem. Phys. Lipids, 201, 50-58 (2016); DOI.
- Favaro, G., Bogialli, S., Di Gangi, I.M., Nigris, S., Baldan, E., Squartini, A., Pastore, P.. and Baldan, B. Characterization of lipopeptides produced by Bacillus licheniformis using liquid chromatography with accurate tandem mass spectrometry. Rapid Commun. Mass Spectrom., 30, 2237-2252 (2016); DOI.
- Feenstra, A.D., O'Neill, K.C., Yagnik, G.B. and Lee, Y.J. Organic-inorganic binary mixture matrix for comprehensive laser-desorption ionization mass spectrometric analysis and imaging of medium-size molecules including phospholipids, glycerolipids, and oligosaccharides. RSC Adv., 6, 99260-99268 (2016); DOI.
- Ferreira, J.P.A., Miranda, I., Gominho, J. and Pereira, H. Chemical characterization of cork and phloem from Douglas fir outer bark. Holzforschung, 70, 475-483 (2016); DOI.
- Flentie, K.N., Stallings, C.L., Turk, J., Minnaard, A.J. and Hsu, F.-F. Characterization of phthiocerol and phthiodiolone dimycocerosate esters of M. tuberculosis by multiple-stage linear ion-trap MS. J. Lipid Res., 57, 142-155 (2016); DOI.
- Foletta, V.C., Palmieri, M., Kloehn, J., Mason, S., Previs, S.F., McConville, M.J., Sieber, O.M., Bruce, C.R. and Kowalski, G.M. Analysis of mammalian cell proliferation and macromolecule synthesis using deuterated water and gas chromatography-mass spectrometry. Metabolites, 6, 34 (2016); DOI.
- Fong, B.Y., Ma, L., Khor, G.L., van der Does, Y., Rowan, A., McJarrow, P. and MacGibbon, A.K.H. Ganglioside composition in beef, chicken, pork, and fish determined using liquid chromatography-high-resolution mass spectrometry. J. Agric. Food Chem., 64, 6295-6305 (2016); DOI.
- Frey, A.J., Feldman, D.R., Trefely, S., Worth, A.J., Basu, S.S. and Snyder, N.W. LC-quadrupole/Orbitrap high-resolution mass spectrometry enables stable isotope-resolved simultaneous quantification and C-13-isotopic labeling of acyl-coenzyme A thioesters. Anal. Bioanal. Chem., 408, 3651-3658 (2016); DOI.
- Furuhashi, T., Nakamura, T., Fragner, L., Roustan, V., Schon, V. and Weckwerth, W. Biodiesel and poly-unsaturated fatty acids production from algae and crop plants - a rapid and comprehensive workflow for lipid analysis. Biotech. J., 11, 1262-1267 (2016); DOI.
- Furukawa, T., Fuda, H., Miyanaga, S., Watanabe, C., Chiba, H. and Hui, S.P. Rapid tin-mediated access to a lysophosphatidylethanolamine (LPE) library: Application to positional LC/MS analysis for hepatic LPEs in non-alcoholic steatohepatitis model mice. Chem. Phys. Lipids, 200, 133-138 (2016); DOI.
- Gachet, M.S. and Gertsch, J. Quantitative analysis of arachidonic acid, endocannabinoids, N-acylethanolamines and steroids in biological samples by LCMS/MS: Fit to purpose. J. Chromatogr. B, 1012, 215-221 (2016); DOI.
- Galliani, G. 1-O-alkylglycerols and fatty acids of cholesteryl esters in squid oil are fully saturated and show parallel relative abundance of chain lengths. A possible compartmented fatty alcohol cycle in squid. Eur. J. Lipid Sci. Technol., 118, 1399-1408 (2016); DOI.
- Gao, F., McDaniel, J., Chen, E.Y., Rockwell, H., Lynes, M.D., Tseng, Y.H., Sarangarajan, R., Narain, N.R. and Kiebish, M.A. Monoacylglycerol analysis using MS/MSALL quadruple time of flight mass spectrometry. Metabolites, 6, 3-25 (2016); DOI.
- Garcia-Reyes, S. and Yanez-Ocampo, G. Microbial biosurfactants: methods for their isolation and characterization. J. Microbiol. Biotechnol. Food Sci., 6, 641-648 (2016); DOI.
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